液相色譜串聯(lián)質(zhì)譜法測(cè)定牛奶中黃體酮?dú)埩袅康牟淮_定度分析

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摘 要：本文采用液相色譜串聯(lián)質(zhì)譜法對(duì)牛奶中黃體酮?dú)埩袅窟M(jìn)行分析測(cè)定。結(jié)果表明，當(dāng)牛奶中黃體酮?dú)埩袅繙y(cè)定含量為6.93 μg·kg-1時(shí)，其擴(kuò)展不確定度達(dá)到1.82 μg·kg-1（k=2）。該方法的不確定度主要來(lái)自校準(zhǔn)過(guò)程產(chǎn)生的不確定度，可對(duì)相關(guān)計(jì)量器具進(jìn)行檢定以改善。

關(guān)鍵詞：黃體酮；液相色譜串聯(lián)質(zhì)譜；牛奶；不確定度

Abstract： This article uses a liquid chromatography tandem mass spectrometry method to determine the residual amount of progesterone in milk. The results showed that when the content of progesterone residue in milk was 6.93 μg·kg-1， the expanded uncertainty reached 1.82 μg·kg-1（k=2）. The uncertainty of this method mainly comes from the uncertainty generated during the calibration process， and relevant measuring instruments can be verified to improve the accuracy

Keywords： progesterone; liquid chromatography tandem mass spectrometry; milk; uncertainty

黃體酮是由雌性的卵巢黃體分泌，是一種孕激素。（剩余6184字）